Extraction and Characterization of Nanocrystalline Cellulose from Sugar Palm Fibres (Arenga Pinnata)

Sally Irvina Ritonga, Erna Frida, Syahrul Humaidi

Abstract


In this work, cellulose was isolated from sugar palm fibre (Arenga pinnata) and converted into sugar palm fibre nanocrystalline cellulose (NCCs) in the hamlet of Medan Sinembah, Indonesia. Alkalization and bleaching were the stages of the therapy process. The cellulose removed with 30 weight percent concentrated sulfuric acid was then used to isolate NCC. Using Fourier transform infrared spectroscopy (FT-IR), the chemical make-up of sugar palm fibre and NCCs was identified. On the basis of structural analysis, X-ray diffraction (XRD) was used. Scanning electron microscopy (SEM) was used for morphological examination, while transmission electron microscopy (TEM) was used to look into NCCs. The outcomes demonstrated that the extracted cellulose underwent bleaching and alkalization processes, respectively, to eliminate lignin and hemicellulose. The diameters of the sugar palm fibre and NCCs were determined 69.025 µm to 6.07±0.14 nm and, respectively

Keywords


Alkalization, Bleaching, Cellulose, Nanocrystalline Cellulose Sugar Palm Fibre

Full Text:

PDF

References


Aini, Z. (2016). Aplikasi Selulosa Whiskers Bagas Tebu Sebagai Penguat Dalam Film Komposit Berbasis PVA/MMT, Tesis, IPB, Bogor.

Aminah, S. (2017). Bionanokomposit Film Berbasis PVA dan Nanoselulosa dari Serat Kenaf (Hibiscus cannabinus L.), Tesis, IPB, Bogor.

Astuti, W.D. (2015). Fabrikasi Komposit Nano fibre selulosa/PVA (Polyvinil Alcohol) Menggunakan Metode Electrospinning, Tesis, UGM, Yogyakarta.

Bachtiar, D., Sapuan, S. M., & Hamdan, M. M. (2008). The effect of alkaline treatment on tensile properties of sugar sugar palm fibre reinforced epoxy composites. Materials & Design, 29(7), 1285–1290. http://dx.doi.org/10.1016/j.matdes.2007.09.006

Bahmid, N. A. (2014). Pengembangan Nano fibre Selulosa Asetat Dari Selulosa Tandan Kosong Kelapa Sawit Untuk Pembuatan Bioplastik, Tesis, IPB, Bogor.

Favier, V., Canova, G. R., Cavaillé, J. Y., Chanzy, H., Dufresne, A., & Gauthier, C. (1995). Nanocomposite materials from latex and cellulose whiskers. Polymers for Advanced Technologies, 6(5), 351–355. http://dx.doi.org/10.1002/pat.1995.220060514

Ilyas, R. A., Sapuan, S.M., Lamin, S.M., & Ridzwan, I.M. (2017). Nanocrystalline cellulose as reinforcement for polymeric matrix nanocomposites and its potential applications: A review. Current Analytical Chemistry, 13. http://dx.doi. org/10.2174/1573411013666171003155624

Ilyas, R.A, Sapuan, S.M. & Ishak, M.R. (2018). Isolation and Characterization of nanocrystalline cellulose from sugar palm fibres (Arenga Pinnata). Carbohydrate Polymers. 181. 1038-1051

Ishak, M. R., Sapuan, S. M., Leman, Z., Rahman, M. Z. A., Anwar, U. M. K., & Siregar, J. P. (2013). Sugar palm (Arenga pinnata): Its fibres, polymers and composites. Carbohydrate Polymers, 91(2), 699–710. http://dx.doi.org/10.1016/j.carbpol.2012. 07.073

Islam, M. T., Alam, M. M., & Zoccola, M. (2013). Review on modification of nanocellulose for application in composites. International Journal of Innovative Research in Science, Engineering and Technology, 2(10), 5444–5451.




DOI: https://doi.org/10.33394/j-ps.v11i2.7935

Refbacks

  • There are currently no refbacks.


Bookmark and Share


Copyright (c) 2023 Sally Irvina Ritonga, Erna Frida, Syahrul Humaidi

Creative Commons License
This work is licensed under a Creative Commons Attribution 4.0 International License.

Creative Commons License
J-PS (Prisma Sains: Jurnal Pengkajian Ilmu dan Pembelajaran Matematika dan IPA IKIP Mataram) p-ISSN (print) 2338-4530, e-ISSN (online) 2540-7899 is licensed under a Creative Commons Attribution 4.0 International License.

View My Stats